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Synthesis, Structure, and Physical Properties of Mixed Valent Mo2SbS2, the First Superconducting Antimonide-Sulfide.

โœ Scribed by Chi-Shen Lee; A. Safa-Sefat; J. E. Greedan; Holger Kleinke

Publisher
John Wiley and Sons
Year
2003
Weight
65 KB
Volume
34
Category
Article
ISSN
0931-7597

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Synthesis, Structure, and Thermoelectric
Synthesis, Structure, and Thermoelectric Properties of the New Antimonide Sulfide MoSb2S
โœ Chi-Shen Lee; Holger Kleinke ๐Ÿ“‚ Article ๐Ÿ“… 2002 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 367 KB ๐Ÿ‘ 2 views

The structure of a new ternary compound, MoSb 2 S, was identified by single-crystal X-ray diffraction. The title compound was synthesized by heating the elements in stoichiometric ratios in sealed silica tubes at 600-800 ยฐC using small amounts of I 2 as a mineralizator. The compound crystallizes in