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Synthesis, structure and magnetism of a tetranuclear Fe(III) complex containing an [Fe4(μ3-O)2]8+ core

✍ Scribed by Phalguni Chaudhuri; Manuela Winter; Peter Fleischhauer; Wolfgang Haase; Ulrich Flörke; Hans-Jürgen Haupt

Publisher
Elsevier Science
Year
1993
Tongue
English
Weight
978 KB
Volume
212
Category
Article
ISSN
0020-1693

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✦ Synopsis

The tetranuclear Fe(III) complex [LFe&-O)&-CHsCOO)a(Sao),Fe,lX

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Hydrothermal Synthesis, Structure, and Magnetic Properties of a Layered Fe(III) Carboxymethylphosphonate: [Fe(H2O)(O3P–CH2–CO2)] or MIL-49
✍ Morgane Sanselme; Myriam Riou-Cavellec; Jean-Marc Grenèche; Gérard Férey 📂 Article 📅 2002 🏛 Elsevier Science 🌐 English ⚖ 412 KB

Fe III (H 2 O)(O 3 P-(CH 2 )-CO 2 )] or MIL-49 was hydrothermally synthesized under autogenous pressure at 1701C for 48 h. Its bidimensional structure was solved from single-crystal X-ray diffraction in the monoclinic space group P2 1 /c (No.14). Cell parameters are a = 9.3836(3) A ˚, b = 6.3798(3)