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Synthesis, structure, and catalytic activity of rhodium complexes with new chiral binaphthyl-based NHC-ligands

✍ Scribed by Haibin Song; Yuqiao Liu; Dongna Fan; Guofu Zi

Book ID: 116680172
Publisher: Elsevier Science
Year: 2011
Tongue: English
Weight: 747 KB
Volume: 696
Category: Article
ISSN: 0022-328X
DOI: 10.1016/j.jorganchem.2011.08.015

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## Abstract Reaction of (__R__)‐bis(pyrrol‐2‐ylmethyleneamino)‐1,1′‐binaphthyl (1H~2~) or (__R__)‐__N__,__N′__‐bis(pyridin‐2‐ylmethyl)‐1,1′‐binaphthyl‐2,2′‐diamine (2H~2~) with Zr(NMe~2~)~4~ (1 equiv.) gives chiral zirconium amides 1‐Zr(NMe~2~)~2~·C~7~H~8~ (4·C~7~H~8~) or 2‐Zr(NMe~2~)~2~ (6) in goo