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Synthesis, Spectroscopy and Tautomeric Study of Thiazoles substituted in positions 2 and 4 by hydroxy, mercapto and amino groups

✍ Scribed by N. Valls; V. M. Segarra; E. Alcalde; A. Marin; J. Elguero

Publisher
John Wiley and Sons
Year
1985
Tongue
English
Weight
728 KB
Volume
327
Category
Article
ISSN
1615-4150

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Axially chiral 1,1′-binaphthyls with non
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Enantiomerically pure hydroxy thiol (S)-(+)-6, amino thiol (S)-(+)-12, and N,N-dimethylamino thiol (S)-(-)-16 have been synthesized from BINOL (S)-(-)-1 and the amino alcohol (S)-(-)-7, respectively, via the Newman-Kwart rearrangement

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## Abstract Broad‐band irradiation (λ > 370 nm) of 2‐hydroxyphenyl azide (1) in Ar at 10K monitored by IR resulted in the formation of at least three major products, all of which were shown to be photointerconvertible under these conditions. The two products showing carbonyl stretching absorption b