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Synthesis, spectroscopic characterization, crystal structures, and theoretical studies of (E)-2-(2,4-dimethoxybenzylidene)thiosemicarbazone and (E)-2-(2,5-dimethoxybenzylidene)thiosemicarbazone

✍ Scribed by Aliakbar Dehno Khalaji; Gholamhossein Grivani; Samaneh Jalali Akerdi; Kazuma Gotoh; Hiroyuki Ishida; Hossein Mighani

Publisher
Springer
Year
2010
Tongue
English
Weight
541 KB
Volume
21
Category
Article
ISSN
1040-0400

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The first syntheses of the novel [1,2]thiaphospholo[4,5-e][1)2,4]triazine ring system, exemplified by the derivatives 3a-c have been accomplished by the action of Lawesson's reagent on the 5-arylmethyl-l,2,4-triazin-6-ones la-Β’, their thiones 2a-c or the Mannich bases 4-6. The structure of these new