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Synthesis and structure of [1,2]thiaphospholo[4,5-e][1,2,4]triazines

โœ Scribed by Yehia A Ibrahim; Azza M Kadry; Maher R Ibrahim; J.N Lisgarten; B.S Potter; R.A Palmer

Publisher
Elsevier Science
Year
1999
Tongue
French
Weight
278 KB
Volume
55
Category
Article
ISSN
0040-4020

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โœฆ Synopsis

The first syntheses of the novel [1,2]thiaphospholo[4,5-e][1)2,4]triazine ring system, exemplified by the derivatives 3a-c have been accomplished by the action of Lawesson's reagent on the 5-arylmethyl-l,2,4-triazin-6-ones la-ยข, their thiones 2a-c or the Mannich bases 4-6. The structure of these new thiaphospholotriazines was established mainly by NMR, and X-ray structural analysis.

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