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Synthesis, Spectroscopic Characteristics, and Crystal Structure of μ-Diphenylsilylene(decacarbonyl)ditungsten Complex (μ-SiPh 2 )W 2 (CO) 10

✍ Scribed by Ga̧dek, Agnieszka; Kochel, Andrzej; Szymańska-Buzar, Teresa

Book ID
126125445
Publisher
American Chemical Society
Year
2003
Tongue
English
Weight
63 KB
Volume
22
Category
Article
ISSN
0276-7333

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The reaction of Na 2 [Fe(CO) 4 ] with Br 2 CF 2 in npentane generates a mixture of the compounds (CO) 3 Fe(l-CO) 3±n (l-CF 2 ) n Fe(CO) 3 (2, n = 2; 3, n = 1) in low yields with 3 as the main product. 3 is obtained free from 2 by reacting Br 2 CF 2 with Na 2 [Fe 2 (CO) 8 ]. The non-isolable monomeri