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Synthesis, physical–chemical, and catalytic properties of mixed compositions Ag/H3PMo12O40/SiO2

✍ Scribed by Yu. Trach; V. Sydorchuk; O. Makota; S. Khalameida; R. Leboda; J. Skubiszewska-Zięba; V. Zazhigalov

Publisher
Springer Netherlands
Year
2011
Tongue
English
Weight
510 KB
Volume
107
Category
Article
ISSN
0022-5215

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Bromohexyl)-3¢,4¢-ethylenedioxy)-2,2¢-bithiophene (3): Into a roundbottomed flask were introduced EDOT (5.9 g, 41.4 mmol) and 150 mL of tetrahydrofuran (THF). The mixture was cooled to ±40 C and butyllithium, 2.5 M in hexanes (19 mL, 47.5 mmol), was added rapidly. After 1 h stirring, tributyltin chl