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Synthesis ofN,N′-bis[4-(1H-1,2,3-triazol-1-yl)furazan-3-yl]-methylenediamine derivatives

✍ Scribed by Batog, L. V.; Rozhkov, V. Yu.; Struchkova, M. I.; Kulikov, A. S.; Makhova, N. N.

Book ID
125368772
Publisher
Springer
Year
2013
Tongue
English
Weight
246 KB
Volume
62
Category
Article
ISSN
1573-9171

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Bis­[4-phenyl-5-(1H-1,2,4-triazol-3-yl)-
Bis­[4-phenyl-5-(1H-1,2,4-triazol-3-yl)-4H-1,2,4-triazol-3-yl] di­sulfide
✍ Pan, Fu-You ;Yang, Jian-Guo ;Chen, Ding-Ben ;Huang, Ling 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 235 KB

The title compound, C 20 H 14 N 12 S 2 , was synthesized by the reaction of 3-hydrazino-1H-1,2,4-triazole with phenyl isocyanate in benzene and by ring closure in an alkaline medium. Intermolecular N-HÁ Á ÁN hydrogen bonds are observed and these form a five-membered ring.