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Synthesis of μ-C2S44− Cobalt Complexes by Activation of the 1,3,4,6-tetrathiapentalene-2,5-dione, and Electrochemical Study of [(Cp*Co)2(μ-C2S4)]

✍ Scribed by Fabrice Guyon; Isabelle V. Jourdain; Michael Knorr; Dominique Lucas; Theresa Monzon; Yves Mugnier; Narcis Avarvari; Marc Fourmigué

Publisher
John Wiley and Sons
Year
2002
Tongue
English
Weight
170 KB
Volume
2002
Category
Article
ISSN
1434-1948

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Treating [Cp\*V(l-Cl) 2 ] 3 (Cp\* = C 5 Me 5 ) and [(2,6-i-Pr 2 C 6 H 3 N) 2 MoMe 2 ], respectively, with Me 3 SnF afforded the title compounds [Cp\*V(l-F) 2 ] 4 (1) and [(2,6-i-Pr 2 C 6 H 3 N) 2 MoF 2 ] ´THF ( 2). 1 has a tetrameric structure, in which four V atoms can be regarded as being arranged