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Synthesis of δ-thiolactams by the aza-Diels–Alder reaction of in situ generated allenyltrimethylsilylthioketenes with imines

✍ Scribed by Shigenobu Aoyagi; Michiko Hakoishi; Mariko Suzuki; Yusuke Nakanoya; Kazuaki Shimada; Yuji Takikawa

Book ID
118501488
Publisher
Elsevier Science
Year
2006
Tongue
French
Weight
145 KB
Volume
47
Category
Article
ISSN
0040-4039

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✍ Takahiko Akiyama; Jun Takaya; Hirotaka Kagoshima 📂 Article 📅 1999 🏛 Elsevier Science 🌐 French ⚖ 197 KB

Three-component aza Diels-Alder reaction, starting from aldehyde, aniline, and Danishefsky's diene, took place smoothly under the influence of HBF4 in aqueous media to afford dihydro-4-pyridone derivatives in high yields.