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Synthesis of α,β-Unsaturated Ketones by Pd-Catalyzed Decarboxylative Allylation of α-Oxocarboxylates

✍ Scribed by Dr. Nuria Rodríguez; Filipe Manjolinho; Matthias F. Grünberg; Prof. Dr. Lukas J. Gooßen


Publisher
John Wiley and Sons
Year
2011
Tongue
English
Weight
238 KB
Volume
17
Category
Article
ISSN
0947-6539

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Synthesis of Ketones from α-Oxocarboxyla
✍ Lukas J. Gooßen; Felix Rudolphi; Christoph Oppel; Nuria Rodríguez 📂 Article 📅 2008 🏛 John Wiley and Sons 🌐 English ⚖ 331 KB 👁 1 views

The experiments in Table 2 were carried out on a 1.00-mmol scale in 20-mL septum-capped vessels. The products were purified by column chromatography (SiO 2 , hexane/ethyl acetate gradient) after aqueous workup.