𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Synthesis of tritium-labelled stobadine, a new cardioprotective agent

✍ Scribed by Vladimir Marko; Jiří Filip; Dušan Uhrín; Tomáš Trnovec; Luděk Beneš

Publisher
John Wiley and Sons
Year
1989
Tongue
French
Weight
269 KB
Volume
27
Category
Article
ISSN
0022-2135

No coin nor oath required. For personal study only.

✦ Synopsis

r e o f P h y s i o l o g i c a l Sciences, S l o v a k Academy o f Sciences, 84216 B r a t i s l a v a , Czechos l o v a k i a . I n s t i t u t e f o r Research, P r o d u c t i o n and A p p l i c a t i o n o f R a d i o i s otopes, R a d i o v h 1, 10227 Prague 10, C z e c h o s l o v a k i a . C h e m i c a l I n s t i t u t e , C e n t r e of C h e m i c a l Research, S l o v a k Academy o f S c i e n c e s , 84238 B r a t i s l a v a , C z e c h o s l o v a k i a . a C SUMMARY 3 S y n t h e s i s o f d i h y d r o c h l o r i d e o f ( -) -c i s -2 , 8 -d i m e t h y l -6 -[ H]-2,3,4, 4a,5,~b-hexahydro-lH-pyrido[4,3b]indole b y c a t a l y t i c r e d u c t i v e d e h a l o g e n a t i o n o f d i h y d r o c h l o r i d e o f (-)-cis-2,8-dimethyl-6-bromo--2,3,4,4a,5,9b-hexahydro-lH-pyrido[4,3b]indole i s d e s c r i b e d t og e t h e r w i t h t h e r e a c t i o n c o n d i t i o n s o f t h e t r i t i a t i o n u s i n g 5:; Pd/BaS04 (UVVVR) i n 0.1 M p h o s p h a t e b u f f e r pH 7.4. S p e c i f i c act i v i t y o f t h e p r o d u c t was 0.9 TBq.mmol-', i t s r a d i o c h e m i c a l p u r i t y

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