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Synthesis of the triazolo[5,1-a][2,4]benzodiazepine ring system

โœ Scribed by Wade, Peter C.; Kissick, Thomas P.; Vogt, B. Richard; Toeplitz, Barbara

Book ID
126286210
Publisher
American Chemical Society
Year
1979
Tongue
English
Weight
609 KB
Volume
44
Category
Article
ISSN
0022-3263

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โœ David W. Knight; Paul B. Little ๐Ÿ“‚ Article ๐Ÿ“… 1997 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 207 KB

Dianion 2 derived from N-Boc-aminobenzotriazole 1 condenses in a [1.2]fashion with ct, fl-unsaturated aldehydes; subsequent oxidation of the resulting allylic alcohols 7 using manganese(IV) oxide or, less effectively, treatment of the derived acetates 10 with Pd(O), results in direct formation of th