A stereoselective one-pot synthesis of p
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Neil Edwards; Jacqueline A. Macritchie; Philip J. Parsons
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Article
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1998
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Elsevier Science
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French
⚖ 186 KB
Treatment of 1,3-bis-[(tert-butyldimethylsilyloxy)ethyl]-1-phenylsulfinyl-1,2-propadiene with aqueous I-IF in acetonitrile :ed to the formation of the rifle compound as one diastereoisomer (from NMR analysis). The reaction was carried out under thermodynamic conditions, and underwent a double deprot