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Synthesis of the C1−C17 Segment of Phorboxazole B

✍ Scribed by Lucas, Brian S.; Luther, Laura M.; Burke, Steven D.

Book ID
125546742
Publisher
American Chemical Society
Year
2004
Tongue
English
Weight
99 KB
Volume
6
Category
Article
ISSN
1523-7060

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✍ Peter Wolbers; Andrea M. Misske; H. Martin R.%Hoffinann 📂 Article 📅 1999 🏛 Elsevier Science 🌐 French ⚖ 209 KB

Two approaches towards an enantiopure C15-C26 segment of the phorboxazoles starting from the corresponding C20-C26 aldehyde are presented. A variety of functionalized oxazoles have been synthesized via the rhodium(lI) acetate catalyzed cycloaddition of dimethyl diazomalonate to substituted nitriles.