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Synthesis of the C16−C28 Spiroketal Subunit of Spongistatin 1 (Altohyrtin A): The Pyrone Approach

✍ Scribed by Crimmins, Michael T.; Katz, Jason D.

Book ID
120377217
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
234 KB
Volume
2
Category
Article
ISSN
1523-7060

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Studies in marine macrolide synthesis: Synthesis of a C16C28 subunit of spongistatin 1 (altohyrtin A) incorporating the CD-spiroacetal moiety
✍ Ian Paterson; Debra J Wallace; Karl R Gibson 📂 Article 📅 1997 🏛 Elsevier Science 🌐 French ⚖ 270 KB

The C! 6-C28 ketone 3, containing the CD-spiroacetal of spongistatin 1 (1), was prepared in 17 steps from aldehyde 9. Both thermodynamic and kinetic conditions were explored for controlling the CD-acetal configuration.