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Synthesis of tertiary 1-alkylthio-l-en-3-yne alcohols

✍ Scribed by A. N. Nikol'skaya; E. P. Levanova; A. N. Volkov; R. N. Kudyakova; K. A. Volkova

Book ID
112487470
Publisher
Springer
Year
1977
Tongue
English
Weight
261 KB
Volume
26
Category
Article
ISSN
1573-9171

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Compound 1 (1.5 g, 7 mmol) was condensed into a 250-mL flask equipped with a PTFE stopcock and containing 4 (0.66 g, 7 mmol). The flask was allowed to stand at room temperature. After 1-2 d, yellow crystals began to collect on the walls of the flask. At intervals of 2-3 d, 7 mmol of I was condensed