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Synthesis of Squalamine Utilizing a Readily Accessible Spermidine Equivalent

✍ Scribed by Zhang, Xuehai; Rao, Meenakshi N.; Jones, Stephen R.; Shao, Bin; Feibush, Penina; McGuigan, Melissa; Tzodikov, Nathan; Feibush, Binyamin; Sharkansky, Ilya; Snyder, Brad; Mallis, Larry M.; Sarkahian, Ani; Wilder, Susan; Turse, Joshua E.; Kinney, William A.; Kjærsgaard, Hans Jørgen; Michalak, Ronald S.

Book ID
126816431
Publisher
American Chemical Society
Year
1998
Tongue
English
Weight
143 KB
Volume
63
Category
Article
ISSN
0022-3263

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✍ Alexander L. Weis; Tamas Bakos; Ivan Alferiev; Xuehai Zhang; Bin Shao; William A 📂 Article 📅 1999 🏛 Elsevier Science 🌐 French ⚖ 118 KB

The synthesis and conversion era new spermidine equivalent (2) to squalamine is reported. It is prepared in a practical manner, is stable to sodium borohydride reduction, is converted to spermidine under mild conditions, and is not prone to internal cyclization reactions.