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Synthesis of Some New 7-Mono and 7, 7-Disubstituted Norbornanes and -Norbornenes. H-NMR Spectrum of 2-Methyl-Spiro (1, 3-Dioxane-5,7′-Norborn-2-Ene

✍ Scribed by E. Bernaert; M. Anteunis; R. De Waele


Publisher
Wiley (John Wiley & Sons)
Year
2010
Weight
333 KB
Volume
82
Category
Article
ISSN
0037-9646

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The reaction of 2,6-diarylidenecyclohexanones with hydrazine hydrate in glacial acetic acid resulted in the formation of diastereomers of (E)-2-acetyl-3-aryl-7-arylidene-3,3a,4,5,6,7-hexahydroindazoles. The relative conÐgurations of these diastereomers were unambiguously assigned using 1H and 13C NM