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Synthesis of some N-[pyridyl(phenyl)carbonylamino]-alkyl-1,2,3,6-tetrahydropyridines

✍ Scribed by Kinfe K. Redda; Hailemichael Melles; Kode Nageswara Rao

Book ID: 112129650
Publisher: Journal of Heterocyclic Chemistry
Year: 1990
Tongue: English
Weight: 504 KB
Volume: 27
Category: Article
ISSN: 0022-152X
DOI: 10.1002/jhet.5570270443

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## Abstract Reaction of isonicotinic [^14^C] acid hydrazide (**1**) with the Zinke salt (**2**) afforded N‐(4‐pyridyl [^14^C] carbonylimino)pyridinium ylide (**3**) in 81% chemical yield. Sodium borohydride reduction of **3** gave N‐(4‐pyridyl [^14^C] carbonylamino) −1,2,3,6‐tetrahydropyridine (**4