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Synthesis of Silylene-Bridged Endohedral Metallofullerene Lu 3 N@ I h -C 80

✍ Scribed by Sato, Kumiko; Kako, Masahiro; Suzuki, Mitsuaki; Mizorogi, Naomi; Tsuchiya, Takahiro; Olmstead, Marilyn M.; Balch, Alan L.; Akasaka, Takeshi; Nagase, Shigeru

Book ID
115455334
Publisher
American Chemical Society
Year
2012
Tongue
English
Weight
705 KB
Volume
134
Category
Article
ISSN
0002-7863

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The discovery of a new isomer of the endohedral metallofullerene Sc 3 N@C 80 is reported. 13 C labeled ($9%) Sc 3 N@C 80 has been synthesized and has been characterized by HPLC, mass spectroscopy and 13 C NMR data. The 13 C NMR spectrum shows six peaks with a 1:2:2:1:1:1 ratio that are assigned to t