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Synthesis of pyridinecarboxylic acidN-oxides and their amides under microwave irradiation conditions

✍ Scribed by D. P. Khrustalev

Book ID
111459966
Publisher
Springer
Year
2009
Tongue
English
Weight
107 KB
Volume
79
Category
Article
ISSN
1070-3632

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Synthesis of oximes, conversion to nitri
Synthesis of oximes, conversion to nitrile oxides and their subsequent 1,3-dipolar cycloaddition reactions under microwave irradiation and solvent-free reaction conditions
✍ BΓ©atrice Touaux; FranΓ§oise Texier-Boullet; Jack Hamelin πŸ“‚ Article πŸ“… 1998 πŸ› John Wiley and Sons 🌐 English βš– 147 KB πŸ‘ 2 views

Aldoximes and ketoximes were readily synthesized from aldehydes and hydroxylamine hydrochloride on Al 2 O 3 without solvent under microwave irradiation. At higher irradiation power, aldoximes dehydrated to nitriles and ketoximes rearranged to amides. Aldoximes reacted in a one-pot reaction with Nchl