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Synthesis of Pyrene and Benzo[ a ]pyrene Adducts at the Exocyclic Amino Groups of 2‘-Deoxyadenosine and 2‘-Deoxyguanosine by a Palladium-Mediated C−N Bond-Formation Strategy

✍ Scribed by Lakshman, Mahesh K.; Ngassa, Felix N.; Bae, Suyeal; Buchanan, Dennis G.; Hahn, Hoh-Gyu; Mah, Heduck

Book ID
125972899
Publisher
American Chemical Society
Year
2003
Tongue
English
Weight
230 KB
Volume
68
Category
Article
ISSN
0022-3263

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The exocyclic amino groups of deoxyadenosine and deoxyguanosine readily add to C-10 of the benzo[a]pyrene 7,8-diol 9,10-epoxides at room temperature overnight in trifluoroethanol. Whereas the dG adducts are obtained as a mixture of cis-and trans-opened diastereomers, the dA adducts arise exclusively

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