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Synthesis of (purin-6-yl)acetates and their transformations to 6-(2-hydroxyethyl)- and 6-(carbamoylmethyl)purines

✍ Scribed by Hasník, Zbyněk; Pohl, Radek; Klepetářová, Blanka; Hocek, Michal

Book ID
120309896
Publisher
UOCHB
Year
2009
Tongue
English
Weight
289 KB
Volume
74
Category
Article
ISSN
0010-0765

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ChemInform Abstract: Synthesis of (Purin
ChemInform Abstract: Synthesis of (Purin-6-yl)acetates and Their Transformations to 6-(2-Hydroxyethyl)- and 6-(Carbamoylmethyl)purines.
✍ Zbynek Hasnik; Radek Pohl; Blanka Klepetarova; Michal Hocek 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 48 KB 👁 2 views

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Synthesis of (purin-6-yl)methylphosphona
Synthesis of (purin-6-yl)methylphosphonate bases and nucleosides
✍ Zbyněk Hasník; Radek Pohl; Michal Hocek 📂 Article 📅 2010 🏛 Elsevier Science 🌐 French ⚖ 318 KB

Three approaches to the synthesis of the title (purin-6-yl)methylphosphonates were investigated and compared. While, the Arbuzov reaction of 6-(iodomethyl)purines with triethyl phosphite did not work, Michaelis-Becker alkylation of the sodium salt of diethyl phosphonate with 6-(mesyloxymethyl)purine