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Synthesis of Pteroylglutamic Acid (Liver L. casei Factor) and Pteroic Acid. I

✍ Scribed by Waller, Coy W.; Hutchings, Brian L.; Mowat, John H.; Stokstad, E. L. R.; Boothe, James H.; Angier, Robert B.; Semb, Joseph; SubbaRow, Y.; Cosulich, Donna B.; Fahrenbach, M. J.; Hultquist, M. E.; Kuh, Erwin; Northey, E. H.; Seeger, Doris R.; Sickels, J. P.; Smith, James M.

Book ID: 121245705
Publisher: American Chemical Society
Year: 1948
Tongue: English
Weight: 486 KB
Volume: 70
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja01181a006

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Pteroylglutamic acid was labeled with deuterium by trifluoroacetic acid-catalyzed exchange with deuterium oxide. The product, pteroylglutamic acid-3',5'-H2, was selectively labeled with deuterium in the 4-aminobenzoyl portion of the molecule; there was no evidence for isotope incorporation at C or