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Synthesis of phosphorylated 1,3,5-oxadiazines via N-acyltrifluoroacetimidoylphosphonates

✍ Scribed by Petro P. Onys'ko; Aleksei A. Sinitsa; Vladimir V. Pirozhenko; Aleksandr N. Chernega

Book ID
102228003
Publisher
John Wiley and Sons
Year
2002
Tongue
English
Weight
150 KB
Volume
13
Category
Article
ISSN
1042-7163

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✦ Synopsis

Abstract

N‐Benzoyl‐ and N‐methoxycarbonyltrifluoroacetimidoylphosphonates react with dimethylcyanamide in a [4+2]‐cycloaddition to give 4‐phosphorylated 1,3,5‐oxadiazines. The structures of the products were confirmed by NMR (^1^H, ^13^C, ^19^F, ^31^P) and IR spectra and by XRD analysis. © 2002 John Wiley & Sons, Inc. Heteroatom Chem 13:22–26, 2002; DOI 10.1002/hc.1102

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