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Synthesis of Phosphoramide Mustard Analogues of Daunomycin and Carminomycin

✍ Scribed by Andrea Csorvási; Katalin E. Kövér; Márta M. Menyhárt; Ferenc Sztaricskai; Yaroslav V. Dobrynin; Tamara G. Nikolaeva

Publisher
John Wiley and Sons
Year
1998
Tongue
English
Weight
75 KB
Volume
331
Category
Article
ISSN
0365-6233

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## Abstract The cyclophosphamide metabolite phosphoramide mustard (PM) was synthesized with isotopic enrichment at each nitrogen and oxygen site. Sequential reaction of __N,N__‐bis(2‐chloroethyl)phosphoramidic dichloride [Cl~2~P(__O__)N(CH~2~CH~2~Cl)~2~] with benzyl alcohol and ammonia gave __N,N__