N-Acetyl-N-methyl-3-aryl-3-[1-(aroyl)ethylthio]-2-propaneamides, prepared from thioaroylketene S,N-acetals, Hg(OAc) 2 and silyl enol ethers of aryl-1-propanones in CH 2 Cl 2 at rt, reacted with NaH in THF to give the title compounds in excellent yields.
✦ LIBER ✦
Synthesis of Novel Alkyl-Sulfanyl 1,3,4-Oxadiazolyl-1,3,5,7-Tetraazatricyclic Ammonium Chloride Type Cationic Surfactants
✍ Scribed by Yıldırım, Ayhan
- Book ID
- 121866651
- Publisher
- Journal of Heterocyclic Chemistry
- Year
- 2014
- Tongue
- English
- Weight
- 232 KB
- Volume
- 52
- Category
- Article
- ISSN
- 0022-152X
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## Abstract Bis‐1,2,3,4‐tetrahydropyrimidinylalkanes/benzenes **2a‐f** have been synthesized by the reaction of N,S‐acetals with formaldehyde and diamines. Reaction of pyrazoles **3a** and **3b** with diamines and formaldehyde yield bis‐4,5,6,7‐tetrahydropyrazolo[3,4‐__d__]pyrimidinylalkanes **4a‐b