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Synthesis of Nitrazepame. Amination of 2-(2-Chloroacetamido)-5-nitrobenzophenone with Hexamethylenetetramine.

✍ Scribed by V. N. Anikeev; A. I. Petrunin; M. T. Kilin; F. V. Guss


Book ID
101965200
Publisher
John Wiley and Sons
Year
2004
Weight
15 KB
Volume
35
Category
Article
ISSN
0931-7597

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✦ Synopsis


Abstract

For Abstract see ChemInform Abstract in Full Text.


πŸ“œ SIMILAR VOLUMES


Synthesis of R2Nξ—ΈR' dissymmetric amines
✍ X. Caillault; Y. Pouilloux; J. Barrault πŸ“‚ Article πŸ“… 1995 πŸ› Elsevier Science 🌐 English βš– 576 KB

The synthesis of methylated tertiary amines (RN( CH3) 2 or R2NCH3) was carried out at low pressure and temperature (P = 0.1 MPa, TI 160Β°C) from fatty nitriles, hydrogen and hexamethylenetetramine (HMTA) over a nickel catalyst. HMTA, the methylating agent, is both very reactive and selective with the