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Synthesis of New, Unnatural Macrocyclic Trichothecenes: 3-isoverrucarin A ((1″-O)(3→4)abeo-verrucarin A), verrucinol, and verrucene. 46th Communication on verrucarins and roridins

✍ Scribed by Nicolas Jeker; Christoph Tamm

Publisher: John Wiley and Sons
Year: 1988
Tongue: German
Weight: 637 KB
Volume: 71
Category: Article
ISSN: 0018-019X
DOI: 10.1002/hlca.19880710808

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✦ Synopsis

Ether 8 as well as the subsequent THP ethers are mixtures of diastereoisomers.

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## Abstract The macrocyclic trichothecene triester 3′‐hydroxy‐2′‐deoxy‐2",3",4",5"‐tetrahydroverrucarin **A** (**37**), has been synthesized starting from the sesquiterpene alcohol verrucarol (**3**), adipic acid and a derivative of mevalonic acid (**14**). The latter has been prepared from 4‐(tetr