Synthesis of New Surfactants Mono and Bipolar Derived from 1,2,4-Triazole-5-thione.
β Scribed by Driss Chebabe; Ahmed Dermaj; Zine El Abidine Ait Chikh; Najat Hajjaji; Isabelle Rico-Lattes; Armand Lattes
- Publisher
- John Wiley and Sons
- Year
- 2005
- Weight
- 20 KB
- Volume
- 36
- Category
- Article
- ISSN
- 0931-7597
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## Abstract The 4,5βdihydroβ1,2,4βtriazole Schiff base derivatives were synthesized with 4βaminoβ4,5βdihydroβ3β(phenoxyβ methyl)β1__H__β1,2,4βtriazoleβ5βthione and substituted benzaldehydes. The chemical structures of the compounds have been confirmed by ^1^H NMR, IR spectra and elemental analysis.
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1,2,4-Triazole-3,5-diamine derivatives were synthesized in moderate to high yields in one-pot reaction from the corresponding isothiocyanates, mono-substituted hydrazines, and sodium hydrogencyanamide, in the presence of 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride. Typically, two tar