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Synthesis of n-methyl-1,3-dimethylbutylamine

✍ Scribed by M. T. Wu

Book ID: 102401916
Publisher: John Wiley and Sons
Year: 1964
Tongue: English
Weight: 122 KB
Volume: 53
Category: Article
ISSN: 0022-3549
DOI: 10.1002/jps.2600530729

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## Abstract The syntheses of 3‐methyl‐4‐phenyl‐3‐butenamide, an hypolipemic compound, labelled 1‐^14^C (VIII) and N,N‐dideutero (XI) are described. The 2‐methyl‐3‐phenyl‐2‐propenyl chloride (VI), reacting with cuprous cyanide‐^14^C, gave the 3‐methyl‐4‐phenyl‐3‐butenonitrile‐1‐^14^C (VII) which, tr