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Synthesis of Mg2FeH6, Mg2CoH5 and Mg2NiH4 by high-pressure sintering of the elements

✍ Scribed by P. Selvam; K. Yvon

Publisher
Elsevier Science
Year
1991
Tongue
English
Weight
215 KB
Volume
16
Category
Article
ISSN
0360-3199

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## Preparation of the Hydrides Mg2FeH6 and Mg2CoH5 by Mechanical Alloying Followed by Sintering. -The production of Mg2FeH6 by the title process is significantly enhanced by milling of 2:1 Mg-Fe powder mixtures under H2 atmosphere followed by sintering at 623 K for 1 day under 50 bar H2 pressure.

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We have designed a new synthesis method for the ternary metal hydride Mg 2 FeH 6 based on the direct reaction of simple hydrides under high-pressure conditions. Well-crystallized samples were prepared in a piston-cylinder hydrostatic press at 2 GPa and temperatures around 750 C from mixtures of MgH