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Synthesis of LiCoO2 starting from carbonate precursors II. Influence of calcination conditions and leaching

โœ Scribed by Anders Lundblad; Bill Bergman


Book ID
104296581
Publisher
Elsevier Science
Year
1997
Tongue
English
Weight
939 KB
Volume
96
Category
Article
ISSN
0167-2738

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โœฆ Synopsis


The effect of initial Li:Co ratio, calcination atmosphere, temperature, leaching in H,O or acetic acid solution on reaction completeness, final Li:Co ratio, primary particle size, conductivity and its sensitivity to different atmospheres has been investigated. The calcination gas composition was found to be very important. A powder with a primary particle size of 100-300 nm and with less than 3 wt.% of unreacted Li,CO, was obtained.


๐Ÿ“œ SIMILAR VOLUMES


Synthesis of LiCoO2 starting from carbon
โœ Anders Lundblad; Bill Bergman ๐Ÿ“‚ Article ๐Ÿ“… 1997 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 756 KB

The reaction mechanisms during calcination of a Li,CO,/Co,O, mixture in air and CO, were monitored by thermogravimetry, differential thermal analysis and complementary calcinations at 300 and 500ยฐC. It was determined how weight reduction, specific surface area and the formation of phases develop. Be