✦ LIBER ✦

Synthesis of LiCoO2 starting from carbonate precursors I. The reaction mechanisms

✍ Scribed by Anders Lundblad; Bill Bergman

Book ID: 104296580
Publisher: Elsevier Science
Year: 1997
Tongue: English
Weight: 756 KB
Volume: 96
Category: Article
ISSN: 0167-2738
DOI: 10.1016/s0167-2738(97)00016-7

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✦ Synopsis

The reaction mechanisms during calcination of a Li,CO,/Co,O, mixture in air and CO, were monitored by thermogravimetry, differential thermal analysis and complementary calcinations at 300 and 500°C. It was determined how weight reduction, specific surface area and the formation of phases develop. Below 400°C the main process is the decomposition of CoCO,. Formation of LiCoO, starts above 400°C but at high 0, partial pressures some Li?CO, seems to react already at 300°C.

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