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Synthesis of Isocyano Peptides by Dehydration of the N-Formyl Derivatives.

✍ Scribed by Gang Zhao; Carine Bughin; Hugues Bienayme; Jieping Zhu

Book ID
101948878
Publisher
John Wiley and Sons
Year
2003
Weight
81 KB
Volume
34
Category
Article
ISSN
0931-7597

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Synthesis, spectroscopy and polymerizati
Synthesis, spectroscopy and polymerization of methyl Ξ±-([13C,15N]isocyano)propionate; acetic formic anhydride as N-formylating reagent
✍ Edward J. Vlietstra; Roeland J. M. Nolte; Jan W. Zwikker; Wiendelt Drenth; Richa πŸ“‚ Article πŸ“… 2010 πŸ› Elsevier Science 🌐 English βš– 567 KB

## Abstract Methyl α‐([^13^C,^15^N]isocyano)propionate was prepared starting from (Β±)‐[^15^N]alanine. The amino acid was converted into the methyl ester, which was formylated with acetic [^13^C]‐formic anhydride, to afford the methyl ester of N‐[^13^C]formyl[^15^N]alanine. Dehydration of the latter