Alkyl azides react with aroyl isothiocyanates at ca 50" to yield I,2,4-dithiazolidines (2) and 1,2,4-thiadiazoles (5). that of p-nitrobenzoyl isothiocyanate. spectral analyses, and, in the case of s, on an X-ray diffraction study. a nearly linear N-S...O arrangement with a S...O distance of 2 . 5 2
β¦ LIBER β¦
Synthesis of heterocycles from aryl isothiocyanates and alkyl azides
β Scribed by L'Abbe, Gerrit; Verhelst, Gabriel; Toppet, Suzanne
- Book ID
- 120997471
- Publisher
- American Chemical Society
- Year
- 1977
- Tongue
- English
- Weight
- 610 KB
- Volume
- 42
- Category
- Article
- ISSN
- 0022-3263
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