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Heterocycles from Acyl Isothiocyanates and Alkyl Azides

✍ Scribed by Gerrit L'abbé; Mitsuo Komatsu; Catherina Martens; Suzanne Toppet; Jean-Paul Declercq; Gabriel Germain; Maurice Van Meerssche

Publisher
Wiley (John Wiley & Sons)
Year
2010
Weight
284 KB
Volume
88
Category
Article
ISSN
0037-9646

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✦ Synopsis

Alkyl azides react with aroyl isothiocyanates at ca 50" to yield I,2,4-dithiazolidines (2) and 1,2,4-thiadiazoles (5).

that of p-nitrobenzoyl isothiocyanate. spectral analyses, and, in the case of s, on an X-ray diffraction study. a nearly linear N-S...O arrangement with a S...O distance of 2 . 5 2 1, indicating no-bond resonance.

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