The synthesis of a hitherto unknown 6 : 5 phase in the quasi-binary system RbCl/PbCl 2 and its structure determination is reported. The compound Rb 6 Pb 5 Cl 16 crystallizes in the tetragonal space group P4/mbm with a large variety of different coordination polyhedra for the cations. Special feature
Synthesis of ferrocenoylphenylureas and the crystal structure of FcCONHCONHC6H5
β Scribed by Li Chen; Qingmin Wang; Runqiu Huang; Chunhui Mao; Jian Shang; Haibin Song
- Publisher
- John Wiley and Sons
- Year
- 2005
- Tongue
- English
- Weight
- 103 KB
- Volume
- 19
- Category
- Article
- ISSN
- 0268-2605
- DOI
- 10.1002/aoc.652
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π SIMILAR VOLUMES
The fluorides CuMoF 6 and CrNbF 6 are triclinic, isostructural with CuSnF 6 . Their crystal structures were solved in the space group P1, by the Rietveld method using the data of their X-ray powder patterns. Both crystal structures can be described as a three-dimensional framework of alternating 6 c
Synthesis and Crystal Structure of Rb 6 Pb 5 Cl 16 . -The hitherto unknown 6:5 phase of title is prepared by reaction of appropriate amounts of RbCl and PbCl 2 (sealed silica tube, 1. 500 β’ C, 0.5 h, 2. 335 β’ C, several weeks). Rb 6 Pb 5 Cl 16 crystallizes in the tetragonal space group P4/mbm (pow