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Synthesis of dl-.alpha.-lipoic acid from a butadiene telomer

✍ Scribed by Tsuji, Jiro; Yasuda, Hideyuki; Mandai, Tadakatsu

Book ID
125952370
Publisher
American Chemical Society
Year
1978
Tongue
English
Weight
296 KB
Volume
43
Category
Article
ISSN
0022-3263

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Civetone is a naturally occurring unique symmetric 17 membered cyclic ketone with the cis double bond. Few synthetic studies for civetone have been attempted. l-5 Stall prepared cis-civetone by separating the cis and trans-mixture. 1 One

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A (;I and B (z), naturally occurring ten-membered lactones which were isolated from the culture filtrate,of Diplodia pinea by Ishida and Wada' and show unique biological activity. A butadiene telomer 3 easily available by palladium catalyzed reaction is a starting material and the method is based on