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Synthesis of Dithiophosphinato Complexes with Bis(diorganothiophilosphoryl)disulfanes: Mo3S7-Cluster Dithiophosphinates

✍ Scribed by Dr. Helmut Keck; Dr. Wilhelm Kuclhen; Dipl.-Chem. Jürgen Mathow; cand. rer. nat. Beate Meyer; Prof. Dr. Dietrich Mootz; Hartmut Wunderlich


Publisher
John Wiley and Sons
Year
1981
Tongue
English
Weight
216 KB
Volume
20
Category
Article
ISSN
0044-8249

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Synthesis, Structure and Characterizatio
✍ S. Lu; Y. Ke; J. Li; Y. Zhang 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 English ⚖ 188 KB 👁 2 views

The complex of (Me 4 N) 2 Mo 3 S 13 (I) has been synthesized under mild hydrothermal condition. The crystal structure was determined by single crystal X-ray diffraction at room temperature. Crystal data: M = 854.91, Trigonal, space group P3 (No. 143), a = 11.2351(8) Å, c = 5.8885(6) Å, and Z = 1, Th