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Synthesis of cyclopentadienylmanganesetricarbonyl from chloromanganesepentacarbonyl and thalliumcyclopentadiene

โœ Scribed by A. N. Nesmeyanov; K. N. Anisimov; N. E. Kolobova

Book ID
112419378
Publisher
Springer
Year
1964
Tongue
English
Weight
54 KB
Volume
13
Category
Article
ISSN
1573-9171

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The preparation of (-)-16 from (+)-3 constitutes a formal enuntiospecific synthesis of (-)-bactobotin from D-glucose. The key traasfonnation involves the diustereoselective addition of LiCHCl2 to 7 in the presence of CeC13. The synthesis of (+)-3 from (+)-uctinobolin sulfate is reported and illustra