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Synthesis of cis-2-aza-3-oxo-4-oxabicyclo[4.2.0]octane and cis-2-aza-3-oxo-4-oxabicyclo[4.1.0]heptane

✍ Scribed by Wheeler, J. W.; Shroff, C. C.; Stewart, Wilford Seabright; Uhm, S. J.


Book ID
126898376
Publisher
American Chemical Society
Year
1971
Tongue
English
Weight
873 KB
Volume
36
Category
Article
ISSN
0022-3263

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The title compound, C~6~H~7~NO~2~, was synthesized from __cis__-1,2-cyclobutanedicarboxylic anhydride by reaction with ammonium acetate under microwave conditions. The crystal structure of the compound shows that the cyclobutane ring is planar with angles ranging from 89.64β€…(12) to 90.37β€…(12)Β°. The