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Synthesis of chiral conformationally fixed cyclohexanones

✍ Scribed by Konopelski, Joseph P.; Djerassi, Carl


Book ID
126179779
Publisher
American Chemical Society
Year
1980
Tongue
English
Weight
686 KB
Volume
45
Category
Article
ISSN
0022-3263

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Synthesis and reduction of chiral sulfin
✍ M.C. CarreΓ±o; J.L.GarcΓ­a Ruano; A. Rubio πŸ“‚ Article πŸ“… 1987 πŸ› Elsevier Science 🌐 French βš– 264 KB

The reaction of cyclohexanone with (S)-(-)-menthyl-p-toluenesulfinate in the presence of Pr@gBr yields a mixture of enantiomerically pure 2-p-tolylsulfinylcyclohexanone diastereoisomers. Their stereoselective reduction to chiral hydroxysulfoxides is also reported. The important role of chiral 8-ket