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Synthesis of characteristic lipopeptides of lipid modified proteins employing the allyl ester as protecting group

✍ Scribed by Schmittberger, Thierry; Cotté, Alain

Book ID
121430414
Publisher
Royal Society of Chemistry
Year
1998
Tongue
English
Weight
84 KB
Volume
8
Category
Article
ISSN
1359-7345

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To a solution of LiAIH, (94.9 mg, 2.5 mmol) in THF (5.0 mL) was added a solution of (R)-BINOL (20 mL. 5.0 mmol, 0.25 M in THF) at 0'C. After 30 min stirring at O'C, this solution of I(O.1 M in THF) was directly used for Michael reactions. 7: To a stirred solution of the catalyst I(0.05 mmol) in THF