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ChemInform Abstract: Enzymatic Synthesis of Peptides and Ras-Lipopeptides Employing Choline Ester as a Solubilizing Protecting, and Activating Group.

✍ Scribed by M. SCHELHAAS; S. GLOMSDA; M. HAENSLER; H.-D. JAKUBKE; H. WALDMANN

Book ID
112030940
Publisher
John Wiley and Sons
Year
2010
Weight
25 KB
Volume
27
Category
Article
ISSN
0931-7597

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Enzymatic Synthesis of Peptides and Ras
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To a solution of LiAIH, (94.9 mg, 2.5 mmol) in THF (5.0 mL) was added a solution of (R)-BINOL (20 mL. 5.0 mmol, 0.25 M in THF) at 0'C. After 30 min stirring at O'C, this solution of I(O.1 M in THF) was directly used for Michael reactions. 7: To a stirred solution of the catalyst I(0.05 mmol) in THF

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Comparative Lipase-Catalyzed Hydrolysis of Ethylene Glycol Derived Esters. The 2-Methoxyethyl Ester as a Protective Group in Peptide and Glycopeptide Synthesis. -The 2-methoxyethyl ester group is found to be a potent protecting group in the synthesis of various peptides and glycopeptides. It can be