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Synthesis of boronated derivatives of pheophorbidea

✍ Scribed by Ol’shevskaya, V. A.; Zaitsev, A. V.; Savchenko, A. N.; Kononova, E. G.; Petrovskii, P. V.; Kalinin, V. N.

Book ID
110160119
Publisher
Springer
Year
2008
Tongue
English
Weight
194 KB
Volume
423
Category
Article
ISSN
0012-5008

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3, -p-carborane-l-yl)propyl]-6-phenyl phenanthridinium chloride hydrochloride (13) has been synthesised by reacting 3,8-diacetamido-6-phenylphenanthridine ) in nitrobenzene at 120°C for 4 days and subsequent removal of the protective groups using 33% HBr/AcOH. Conversion to the chloride hydrochlori