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Synthesis of bis(1,3-dihydroxy-isopropyl)amine by reductive amination of dihydroxyacetone: Open chain equivalent of DMDP and a potential AB4 dendritic monomer

✍ Scribed by David A. Scott; Thomas M. Krülle; Malcolm Finn; Robert J. Nash; Ana L. Winters; Naoki Asano; Terry D. Butters; George W.J. Fleet

Publisher: Elsevier Science
Year: 1999
Tongue: French
Weight: 290 KB
Volume: 40
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(99)01611-1

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Bis(1,3-dihydroxy-isopropyl)amine (BDI)

Bis(1,3-dihydroxy-isopropyl)amine (BDI) as an AB4 dendritic building block: rapid synthesis of a second generation dendrimer

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Bis(1,3-dihydroxy-isopropyl)amine (BDI) 1, a symmetrical AB 4 dendritic building block, is developed into two diamine linkers in which the nitrogen is more nucleophilic. The four primary alcohols in BDI undergo Michael reactions with t-butyl acrylate. Branch cells of this rare multiplicity allow the