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Synthesis of a Square Pyramidal Tungsten(VI) Alkylidene Complex with a Bis(Amide) Chelate Ligand

✍ Scribed by VanderLende, Daniel D.; Abboud, Khalil A.; Boncella, James M.

Book ID: 125522389
Publisher: American Chemical Society
Year: 1994
Tongue: English
Weight: 342 KB
Volume: 13
Category: Article
ISSN: 0276-7333
DOI: 10.1021/om00021a002

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## Abstract The bidentate ligand 2,11‐bis(diphenylphosphinomethyl)benzo[__c__]phenanthrene (**1**) was synthesized from 2,11‐dimethyl‐benzo[__c__]phenanthrene (**3**) __via__ the corresponding bromomethyl derivative **9. 3** was obtained from the cyclization with boron trifluoride etherate of 1,1‐d